Table 3.
Validation parameters such as limit of detection (LOD), limit of quantification (LOQ) and recover ies of pesticides detected in vegetables

Pesticides Commodity Range (μg/mL) Correlation coefficient(r2) LOD (mg/L) LOQ (mg/L) Recovery (%)
Procymidone cabbage 0.02-10 0.9992 0.02 0.07 97.6 ± 2.3
leek 0.02-10 0.9984 0.02 0.07 95.3 ± 3.0
red beet 0.02-10 0.9999 0.03 0.10 97.7 ± 2.8
Endosulfan spinach 0.02-10 0.9923 0.02 0.07 92.8 ± 4.8
cabbage 0.02-10 0.9992 0.02 0.07 93.7 ± 2.2
chwinamul 0.02-10 0.9992 0.02 0.07 92.5 ± 3.5
Azoxystrobin chwinamul 0.02-10 0.9998 0.05 0.17 82.5 ± 5.2
Diethofencarb perilla leaves 0.02-10 0.9980 0.03 0.10 98.3± 4.1
crown daisy 0.02-10 0.9991 0.03 0.10 101.4 ± 2.2
Chlorfenapyr green pepper 0.02-10 0.9999 0.02 0.07 98.7 ± 2.0
leek 0.02-10 0.9999 0.02 0.07 103.1 ± 1.5
Dimethomorph spinach 0.02-10 0.9949 0.03 0.10 91.6 ± 3.4
cabbage 0.02-10 0.9992 0.03 0.10 86.3 ± 1.4
Cypermethrin lettuce 0.02-10 0.9983 0.03 0.10 88.2 ± 1.8
leek 0.02-10 0.9990 0.03 0.10 90.7 ± 1.3
Diniconazole perilla leaves 0.02-10 0.9999 0.02 0.07 98.6 ± 2.1
Carbendazim perilla leaves 0.02-10 0.9995 0.05 0.17 89.6 ± 5.2
Chlorothalonil cucumber 0.02-10 0.9999 0.05 0.17 96.4 ± 4.4
Tebufenpyrad perilla leaves 0.02-10 0.9995 0.02 0.07 97.2 ± 3.0
Ethoprophos green pepper 0.01-10 0.9981 0.01 0.04 90.6 ± 2.5
Tetraconazole green pepper 0.02-10 0.9999 0.02 0.07 98.4 ± 2.4
Carbofuran perilla leaves 0.02-10 0.9945 0.05 0.17 90.2 ± 4.0
Pyridalyl cabbage 0.02-10 0.9995 0.02 0.07 93.6 ± 3.2
Phorate chwinamul 0.02-10 0.9946 0.02 0.07 96.1 ± 1.8
Chlorfluazuron chwinamul 0.02-10 0.9994 0.03 0.10 98.2 ± 1.9
Fludioxonil spinach 0.02-10 0.9988 0.05 0.17 95.5 ± 2.8