Table 2. Experimental conditions for coffee aroma analysis by GC-IMS

conditions
GC Autosampler Headspace vial 20 mL
Incubation time 20 min
Sample amount 0.3 g
Incubation temperature 70℃
Injector temperature 80℃
Syringe temperature 80℃
Sample amount 100 μL
Agitation speed 400 rpm
GC Column Capillary column non-polar column constituted by 94% methyl, 5% phenyl, 1% vinyl silicone
Length of column 15 m
ID of column 0.32 mm
Column temperature 80℃
Runtime 30 min
IMS Ionization source Tritium 100 MBq
Voltage Positive drift
Carrier gas flow(N2 gas) 1 mL/min 2 min -> 20 mL/min 15 min -> 20 mL/min 20 min -> 1 mL/min 22 min -> 11 mL/min 30 min
Drift gas flow(N2 gas) 150 mL/min
Drift tube temperature 45℃