conditions | ||
---|---|---|
GC Autosampler | Headspace vial | 20 mL |
Incubation time | 20 min | |
Sample amount | 0.3 g | |
Incubation temperature | 70℃ | |
Injector temperature | 80℃ | |
Syringe temperature | 80℃ | |
Sample amount | 100 μL | |
Agitation speed | 400 rpm | |
GC Column | Capillary column | non-polar column constituted by 94% methyl, 5% phenyl, 1% vinyl silicone |
Length of column | 15 m | |
ID of column | 0.32 mm | |
Column temperature | 80℃ | |
Runtime | 30 min | |
IMS | Ionization source | Tritium 100 MBq |
Voltage | Positive drift | |
Carrier gas flow(N2 gas) | 1 mL/min 2 min -> 20 mL/min 15 min -> 20 mL/min 20 min -> 1 mL/min 22 min -> 11 mL/min 30 min | |
Drift gas flow(N2 gas) | 150 mL/min | |
Drift tube temperature | 45℃ |