Table 1. Recovery, limits of detection (LOD) and limits of quantification (LOQ) for mycotoxins analyzed
| Mycotoxins1) | Recovery2)±RSD3) (%) | LOD (μg/kg) | LOQ (μg/kg) |
| Spiked level 1 | Spiked level 2 |
| AFB1 | 94.2±0.4 | 84.0±5.5 | 0.1 | 0.3 |
| AFB2 | 94.8±0.5 | 85.1±4.7 | 0.07 | 0.22 |
| AFG1 | 93.1±1.3 | 78.0±13.1 | 0.1 | 0.4 |
| AFG2 | 86.9±1.0 | 71.9±9.5 | 0.08 | 0.23 |
| OTA | 98.4±4.1 | 100.1±6.9 | 2 | 7 |
| PAT | 90.2±0.6 | 83.4±1.8 | 5 | 15 |
| FB1 | 94.2±5.3 | 71.5±7.2 | 7 | 20 |
| FB2 | 92.1±7.5 | 83.8±8.5 | 7 | 20 |
AFB1, B2, G1 and G2, aflatoxin B1, B2, G1 and G2; OTA, ochratoxin A; PAT, patulin; FB1 and FB2, fumonisin B1 and B2.
AFB1 and G1, 50 μg/kg (spiked level 1) and 100 μg/kg (spiked level 2); AFB2 and G2, 12.5 μg/kg and 25 μg/kg; OTA, 200 and 400 μg/kg; PAT: 1,000 and 2,000 μg/kg; FB1 and FB2, 1,000 and 4,000 μg/kg.
RSD, relative standard deviation (n=3 replicates).