Table 1. Linearity and limits of detection and quantification of the vitamin K analysis using enzymatic extraction coupled with HPLC-FLD
Analytes | Regression equation1) | Correlation coefficient (R2) | LOD2) (μg/100 g) | LOQ3) (μg/100 g) |
Phylloquinone | y=508.25x-0.0837 | 0.9999 | 0.017 | 0.040 |
Menaquinone | y=511.58x-0.0927 | 0.9999 | 0.021 | 0.052 |
y and x of the regression equation for phylloquinone and menaquinone indicate peak area (mAU) of HPLC chromatograms and the concentration of corresponding analytes, respectively.
Limit of detection.
Limit of quantification.